In Situ Visualization and Quantification of 1–100 μm Micro-Cracks in Cementitious Materials via Contact Sponge–Fluorescence Tracing: Mechanism of Aggregation-Caused Quenching

This paper proposes an innovative contact sponge–fluorescent tracer technique for the rapid, non-destructive detection of 1–100 μm microcracks in cementitious materials. The technique combines a porous sponge carrier with a moisture-sensitive fluorescent tracer: after the sponge adsorbs the aqueous dye solution, capillary action drives fluorescent molecules into microcracks upon contact with the wall, ensuring stable luminescence during a 30-day continuous observation period. This technique was applied to cement paste specimens with three different water-to-cement ratios, dried at 105 °C for varying durations to induce drying–shrinkage microcracks. Results demonstrate that the technique clearly characterizes microcrack networks with high resolution and excellent stability. Under the same drying duration, the average microcrack width decreases with an increasing water-to-cement ratio, while the total crack length and fractal dimension increase. Regression analysis reveals that the average crack width is the primary factor controlling capillary water absorption. This method enables the early detection of microcracks in critical infrastructure such as tunnels and bridges, facilitating timely maintenance and reducing deterioration risk.