The development of echium oil-loaded nano-microcapsules by electrospraying, mono- and coaxial spray-drying was investigated. Brewers' spent grains (BT) or defatted grape seed flour (GT) hydrolysates were used as plant-based emulsifiers. The oxidative stability of the capsules was assessed by Electron Spin Resonance (ESR). Electrosprayed particles had narrow size distribution, mostly 80%), showing higher oxidative stability. BT, exhibiting higher emulsifying capacity and leading to more viscoelastic interfacial films than GT, led to microcapsules with higher oxidative stability with no difference between mono- and coaxial processes. In contrast, coaxial spray-drying, resulting in capsules with core-shell structure, reduced oil leakage when using the less powerful emulsifier GT, enhancing oxidative stability when compared to the monoaxial process. • Echium oil was encapsulated by electrospraying and mono- or coaxial spray-drying. • Brewers' spent grain and defatted grape seed hydrolysates were studied as emulsifiers. • Capsules with brewers' spent grain hydrolysate showed higher oxidative stability. • Spray-dried capsules showed higher oxidative stability than electrosprayed capsules. • Coaxial spray-drying enhanced oxidative stability of grape hydrolysate capsules.
Bisinotto et al. (Sun,) studied this question.