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On a preparative scale of 10 mg per batch the dioxirane 2 can be synthesized from the diazomethane 1. Compound 2 is the first dioxirane that is stable in the solid state at room temperature. An intermediate, probably the carbonyl oxide, can also be kept for several hours in solution at –78°C.
Kirschfeld et al. (Thu,) studied this question.
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