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High-resolution electron microscopy shows the coexistence of several distinct core structures for coincident-site lattice boundaries in NiO bicrystals near =5, (310), and =13, (510), where is the reciprocal density of coincident lattice sites. Lattice expansion perpendicular to the =5 grain boundaries is considerably smaller than calculated theoretically. Structural units in boundaries near =13, (510) exhibit translations normal to the grain-boundary plane, resulting in a rumpling of the interface on an atomic scale. Our observations suggest the presence of a high concentration of Schottky pairs in the grain boundaries.
Merkle et al. (Mon,) studied this question.
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