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The design and operation of a low temperature vacuum calorimeter which is internally cooled from 13° to 2°K is described. The principle employed is that of adiabatically expanding cooled helium gas from a small pressure chamber, located inside the calorimeter can. The heat capacities of crystalline benzene and methyl alcohol and crystalline and glassy glycerol have been measured down to 3°K. New values of the entropies of these substances at various temperatures have been calculated. Below 9°K the heat capacity of glassy glycerol is 100 percent larger than that of crystalline glycerol. The glassy form apparently has 4.64 units of entropy at the absolute zero.
Ahlberg et al. (1937) studied this question.