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A regio-/chemoselective silylmetalation of various functionalized alkenes based on the zinc silyl complex in the presence of a catalytic amount of copper cyanide was developed. Silylmetalation of alkenes, followed by electrophilic trapping, proved to be a powerful tool for the functionalization of the continuous carbon atoms of the alkenes. The resultant alkylsilanes can be converted smoothly into alcohols by oxidative cleavage of the carbon−silicon bond.
Nakamura et al. (Fri,) studied this question.
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