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Bulk specimens (0.4–4 g mass) of the alloy Pd40Ni40P20 have been undercooled consistently to the glass state, with no detectable superficial crystallinity, in a molten flux of dehydrated boron oxide. The minimum dimension of the most massive glass specimen, so formed, was 1.0 cm. The absence of crystallinity in the specimens was confirmed by x-ray diffraction, scanning electron microscopy, and calorimetry.
Kui et al. (Sat,) studied this question.
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