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A continuous nitrogen-flow cooling device, generally applicable to X-ray diffraction studies, is described. The device works in the range 77.4 to 323.0 K with a precision of ±0.1 K and a liquid-nitrogen constant consumption rate of 0.5 l h−1 over the whole temperature range. The supply vessel is unpressurized, so that refilling can be done without any observable influence on the cooling of the sample.
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Cosier et al. (Tue,) studied this question.
synapsesocial.com/papers/69dd672a2f737f012599be8c — DOI: https://doi.org/10.1107/s0021889886089835
J. Cosier
University of Ljubljana
A. M. Glazer
John Innes Centre
Journal of Applied Crystallography
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