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A well-defined silica-supported molybdenum dioxo species, (triple bond, length as m-dashSiO)2Mo(O)2, is prepared by grafting Mo(O)2OSi(OtBu)32 on partially dehydroxylated silica SiO2-700, followed by thermal treatment under high-vaccum and calcination. Activated by an organosilicon agent the resulting material is active for olefin metathesis at 30 °C.
Yamamoto et al. (Mon,) studied this question.
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