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Brookite TiO2 mesocrystals were synthesized for the first time using amorphous titanate used as a precursor, exhibiting a high rate capability when applied as an anode for lithium-ion batteries. An in situ X-ray diffraction test of lithium intercalation into the brookite TiO2 structure was further investigated and revealed a reversible phase transformation.
Zhang et al. (2018) studied this question.