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The function of advanced characterization methods in materials science is discussed in this review article, which primarily focuses on how these methods are used in structural composites, energy storage materials, and semiconductors. Discovering the intricate chemical and structural features of these materials has been greatly aided by the combination of methods like scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffraction (XRD), and Fourier-transform infrared spectroscopy (FTIR). Understanding materials’ thermal stability and behavior under operating settings is essential for maximizing performance. Technology such as thermogravimetric analysis (TGA) and differential scanning calorimetry (DSC) have further contributed to this understanding. A key area where in situ and operando characterization techniques are becoming increasingly important is the study of energy storage devices. Researchers can gain invaluable insights into degradation mechanisms and failure points by monitoring real-time material changes under working conditions. The interaction of a material’s thermal, chemical, and structural characteristics can be better understood when spectroscopy and microscopy are used together. This study focuses on a significant material characterization trend involving combining high-throughput screening with machine learning (ML) and artificial intelligence (AI). AI can shorten the time it takes from ideation to implementation by improving the accuracy and speed of material discovery using massive data sets produced by sophisticated methods. Researchers can better anticipate material behavior using this data-driven method, particularly in operational or severe situations that are hard to replicate experimentally. Researchers in the field of materials science have concluded that improving characterization methods is crucial to the field’s future progress. Critical will be multidimensional and hybrid approaches that integrate several types of analysis. In addition, studying and forecasting the behavior of next-gen materials, especially those used in energy storage, semiconductor technology, and nanocomposites, will rely heavily on AI-driven research. New opportunities for creating sustainable, high-functioning materials will arise because of these advancements.
Patel et al. (Fri,) studied this question.