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September 5, 2025Journal of the American Chemical Society

Enantioselective Radical–Radical Cross-Couplings of β-Hydroxy Amides and N-Hydroxyphthalimide Esters via Ni/Photoredox Catalysis

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Authors

LZLi-Li ZhangLLLianjie LiNWNing Wang

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Overview

This research demonstrates enantioselective coupling of alkyl chains using photoredox and nickel catalysis, highlighting its application in synthesizing valuable molecules.

Key Points

  • This method achieves efficient enantioselective transformations of alkyl radicals, resulting in enantioenriched products.
  • The approach connects photoredox and nickel catalysis to control the selectivity of radical reactions, an advancement in organic synthesis.
  • A one-pot process includes generating N-hydroxyphthalimide in situ, simplifying the overall synthetic route for complex scaffolds.
  • Comprehensive mechanistic studies outline a Ni(I)/Ni(II) cycle integral to achieving controlled radical couplings.

Cite This Study

Zhang et al. (2025) studied this question.

synapsesocial.com/papers/68bb3edf2b87ece8dc956d57https://doi.org/10.1021/jacs.5c10963
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