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In this communication we describe a technique for measuring the absolute quantum yields (QYs) of upconverting nanomaterials based on the use of a commercially available fluorimeter and an integrating sphere. Using this setup, we have successfully acquired luminescence efficiency data (pump laser, absorbed pump, and visible emitted intensities) for lanthanide-doped upconverting nanoparticles. QYs in the range of 0.005% to 0.3% were measured for several NaYF(4): 2% Er(3+), 20% Yb(3+) nanoparticles with particle sizes ranging from 10 to 100 nm while a QY of 3% was measured for a bulk sample.
Boyer et al. (Fri,) studied this question.