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The simple and cost‐effective co‐precipitation method is used for the synthesis of pure Co 3 O 4 and 5% Sn‐doped Co 3 O 4 nanoflakes. Crystallographic parameters, chemical composition, morphological properties, optical properties, and surface area are analyzed using X‐ray diffraction data (XRD), Fourier transform infrared spectroscopy (FT‐IR), Raman analysis, UV–vis, field emission scanning microscopy, energy‐dispersive X‐ray analysis, and Brunauer–Emmett–Teller (BET), respectively. By using cyclic voltammetry and electrochemical impedance spectroscopy in a 2 m KOH electrolyte, the electrochemical characteristics of both pure and 5% Sn‐doped Co 3 O 4 are verified. The sample results show that the presence of Sn 2+ has an impact on surface area, band gap, specific capacitance, and electrochemical performance of Co 3 O 4 . According to XRD data, synthetic material has a cubic structure. The surface area of the sample is scrutinized using BET which exhibits a higher surface area of 1084.998 m 2 g −1 than pure Co 3 O 4 (92.842 m 2 g −1 ) demonstrating that enhancement in surface area as dopant concentration increases. It is observed that porous 5% Sn‐doped Co 3 O 4 nanoflakes has the higher specific capacitance, i.e., 203.6 F g −1 with a high surface area. It is well noticed that drastic change in specific capacitance with 5% Sn doping. These observations and experiments reveal that designed electrode is a promising candidate for supercapacitor application.
Sonpir et al. (2024) studied this question.