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February 8, 20260 citationsOpen Access

Synthesis and Characteristics of New 3-(Dichloromethyl)-2-nitro-6,7-dihydro-1-benzofuran-4(5H)-ones

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IPIlia A PilipenkoHerzen UniversityOOOlga Yu. OzerovaHerzen UniversityODOleg P. DemidovNorth-Caucasus Federal University

Key Points

  • To synthesize and characterize new 3-(dichloromethyl)-2-nitro-6,7-dihydro-1-benzofuran-4(5H)-ones.
  • Synthesis of the compounds via organic chemical techniques.
  • Single-crystal X-ray diffraction for structural analysis.
  • 1H, 13C-{1H}, 1H-13C HMQC and HMBC NMR spectroscopy for characterization.
  • Infrared (IR) spectroscopy for functional group identification.
  • Ultraviolet (UV) spectroscopy for analyzing electronic transitions.
  • New compounds were successfully synthesized and characterized.
  • Structural characteristics were confirmed through various spectroscopy techniques.
  • The absence of previously known compounds indicates originality in the synthesis.

Abstract

The previously unknown compounds—3- (dichloromethyl) -2-nitro-6, 7-dihydro-1-benzofuran-4 (5H) -ones—have been synthesized and structurally characterized via single-crystal X-ray diffraction, 1H, 13C–1H, 1H–13C HMQC and 1H–13C HMBC NMR spectroscopy, IR, and UV spectroscopy.

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Cite This Study

Pilipenko et al. (2026) studied this question.

synapsesocial.com/papers/6988291e0fc35cd7a884920fhttps://doi.org/10.3390/m2134
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