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March 10, 2026ChemistrySelect1 citations

Carbon Paste Electrode Developed From Recycled Manganese Oxide From Batteries and Its Application in the Electrochemical Detection of Paracetamol

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GCGloria A. Cosco‐SalgueroÉNÉdgar NaglesJAJorge Angulo‐Cornejo

Key Points

  • To develop and evaluate a carbon paste electrode using recycled manganese oxide for the electrochemical detection of paracetamol.
  • Recycled manganese oxide sourced from used D-type batteries was used to fabricate a carbon paste electrode.
  • Electrochemical detection of paracetamol was performed using cyclic voltammetry and square wave voltammetry techniques.
  • Characterization of the electrode properties was conducted via SEM, EDS, x-ray diffraction, FTIR, and Raman spectroscopy.
  • The developed electrode achieved a detection limit of 0.06 µmol/L for paracetamol.
  • High selectivity over other substances was observed in real samples containing paracetamol.
  • The electrode was produced without the need for cleaning or purification of the recycled material.

Abstract

ABSTRACT The reuse of used battery components promotes a circular economy and reduces the need to extract compounds from nature and the costs associated with designing new materials. This work reports the use of recycled compounds from batteries with great potential for application in the development of modified electrodes. In this case, manganese oxide was recycled from a D‐type battery, and with this material, a simple and economical working electrode with electrooxidative activity was manufactured for the detection of paracetamol. With this modified electrode, a detection limit of 0.06 µmol/L was obtained, with great selectivity over other substances present in real samples containing paracetamol. The characteristics of the electrode, such as its surface and electrochemical activity, were analyzed via SEM, EDS, x‐ray diffraction, FTIR and Raman spectroscopy, cyclic voltammetry, and square wave voltammetry. Also, that recycled battery material was used without the need for cleaning or purification, which makes it easy to handle.

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Cite This Study

Cosco‐Salguero et al. (2026) studied this question.

synapsesocial.com/papers/69af957570916d39fea4d158https://doi.org/10.1002/slct.202505822
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