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March 25, 2026Coatings2 citationsOpen Access

Tailoring Lithium-Ion Battery Separator Performance Through Cellulose Selection: A Comparative Analysis of Microcrystalline, Nanofibrillated, and Bacterial Cellulose Coatings

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XSXinyu SongHMHuiling MoAZAnqi Zhou

Key Points

  • This research aims to investigate how different cellulose configurations affect lithium-ion battery separator performance.
  • Construction of functionalized polypropylene composite separators using microcrystalline, nanofibrillated, and bacterial cellulose.
  • Utilization of vacuum filtration for coating application.
  • Comparison of contact angle measurements and electrochemical performance metrics.
  • Contact angles decreased significantly, enhancing interfacial affinity to below 10°.
  • MCC@PP showed the highest lithium-ion migration number of 0.41.
  • Capacity retention rate for MCC@PP reached 88.04% after 100 cycles at 0.5 A/g.

Abstract

The inherent hydrophobicity of polyolefin separators significantly impedes rapid electrolyte wetting, thereby limiting the electrochemical performance of lithium-ion batteries. Cellulose, as a hydroxyl-rich natural polymer, serves as an ideal material for enhancing the interface properties of separators. However, there is still a lack of systematic understanding regarding how the morphological structures of cellulose (such as granular, fibrous, or network-like forms) influence the coating structure and ion transport mechanisms. Here, three representative cellulose derivatives—microcrystalline cellulose (MCC), cellulose nanofibers (CNF), and bacterial cellulose (BC)—were selected to construct functionalized polypropylene (PP) composite separators through vacuum filtration. Experimental results demonstrate that all three cellulose coatings reduced contact angles from 50.8° to below 10°, significantly enhancing interfacial affinity. Systematic comparison reveals that cellulose configuration decisively influences separator performance: unlike the dense fiber entanglement networks formed by CNF and BC, the unique rigid granular packing structure of MCC maintains hydrophilicity while establishing more permeable ion transport pathways. Among these, MCC@PP exhibited optimal electrochemical performance, with the lithium-ion migration number increasing to 0.41 and a capacity retention rate of 88.04% after 100 cycles at 0.5 A/g. This study elucidates the relationship between cellulose configuration and the modification of separator performance, demonstrating that MCC represents a more efficient, robust, and cost-effective option for separator modification compared to complex fiber networks.

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Cite This Study

Song et al. (2026) studied this question.

synapsesocial.com/papers/69c37be2b34aaaeb1a67eabdhttps://doi.org/10.3390/coatings16030391
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