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April 17, 2026Ain Shams Engineering Journal0 citationsOpen Access

Utilization of rice husk ash for sustainable synthesis of titania nanoparticles on ordered SBA-15 mesopores with high photoactivity and stability

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TLTzong-Horng LiouYLYen‐Tung LinMing Chi University of TechnologyCWChi-En WuMing Chi University of Technology

Key Points

  • The aim is to develop a sustainable photocatalyst from rice husk ash to degrade Congo red in wastewater.
  • Synthesis of SBA-15-supported TiO2 using rice husk ash as precursor
  • Characterization of textural parameters
  • Photocatalytic experiments under near-ultraviolet light
  • Stability and recycling tests of the catalyst
  • Achieved nearly complete degradation of Congo red within 120 minutes
  • Optimal conditions include 30 wt% TiO2 and a calcination temperature of 900 °C
  • Formation of Si–O–Ti bonds enhanced photocatalytic efficiency
  • Textural parameters ranged from 156-327 m2/g and 7.51-9.58 nm pore sizes

Abstract

Rice husks (RHs) are an agricultural waste. Currently, the waste is not effectively utilized, resulting in environmental pollution. This study is focused on the SBA-15-supported TiO 2 catalyst fabricated from RH ash (RHA) as a novel material for near-ultraviolet-light degradation of Congo red (CR). Experimental results show that the formation of new Si–O–Ti bonds was beneficial to photocatalytic reaction. The textural parameters of catalysts were in the ranges of 156–327 m 2 /g, 0.204–0.462 cm 3 /g, and 7.51–9.58 nm. The optimal catalytic conditions were a TiO 2 content of 30 wt%, calcination temperature of 900 °C, solution pH of 1, composite dosage of 50 mg, and initial CR concentration of 40 ppm. Nearly complete degradation was achieved within 120 min. The kinetics analysis, degradation mechanism, and stability of the recycled catalyst were also explored in depth. Recycling RHA to prepare mesoporous photocatalysts can simultaneously treat biowaste and purify wastewater and has high economic value.

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Cite This Study

Liou et al. (2026) studied this question.

synapsesocial.com/papers/69e1cf985cdc762e9d8587achttps://doi.org/10.1016/j.asej.2026.104182
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