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May 15, 2026Applied Sciences0 citationsOpen Access

Data Acquisition System for the Tender-Energy Spectroscopy Beamline at the Shanghai Synchrotron Radiation Facility

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YZY ZHAOWZW. J. ZhuLGLingling Guo

Key Points

  • This work aims to develop and validate a data acquisition system for enhanced X-ray spectroscopy at a specific beamline.
  • Developed a distributed architecture integrating EPICS hardware control with Bluesky for experiment orchestration.
  • Implemented hardware-level synchronization between a silicon drift detector and multichannel scaler for precise timing.
  • Validated system performance using standard reference samples to acquire various XANES and EXAFS spectra.
  • Successfully acquired high-quality Cl K-edge XANES spectra and Co K-edge EXAFS data with extended k-space coverage (up to 16 Å−1).
  • Achieved high-sensitivity Ti K-edge fluorescence XAFS on dilute TiO2 samples, confirming system reliability.
  • Confirmed the system's capability for high-precision spectroscopy across the tender-energy range of 2–16 keV.

Abstract

A dedicated data acquisition system has been developed and commissioned for the tender-energy spectroscopy beamline BL16U1 at the Shanghai Synchrotron Radiation Facility. The system implements a distributed architecture integrating EPICS-based hardware control with the Bluesky experiment orchestration environment, supporting multiple X-ray absorption spectroscopy modes including transmission, total electron yield, total fluorescence yield, and partial fluorescence yield detection. A key technical feature is the hardware-level synchronization between a multi-channel silicon drift detector and a multichannel scaler, enabling precise timing for fluorescence-XAS measurements. A unified graphical interface based on Control System Studio provides streamlined experiment control and real-time data visualization. System validation using standard reference samples demonstrates successful acquisition of high-quality Cl K-edge XANES spectra in fluorescence mode, high signal-to-noise Co K-edge EXAFS data in transmission mode with extended k-space coverage up to 16 Å−1, and high-sensitivity Ti K-edge fluorescence XAFS on dilute (1–3%) TiO2 polymorphs. These results confirm the system’s capability for reliable, high-precision spectroscopy across the tender-energy range (2–16 keV), supporting both trace-element analysis and detailed local-structure determination. The fully integrated system is now operational at the beamline, providing a robust platform for advanced X-ray absorption studies in environmental, catalytic, and materials science.

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Cite This Study

ZHAO et al. (2026) studied this question.

synapsesocial.com/papers/6a06b83de7dec685947aaca7https://doi.org/10.3390/app16104751
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