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May 26, 2026Materials0 citationsOpen Access

Factorial Optimization of Secondary Annealing Parameters for Enhanced Magnetic Performance in M4 Grain-Oriented Electrical Steel Toroidal Cores

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AMAlma Lilia Moreno-RíosLZLuis Adrian Zuñiga-AvilesJRJosé Martin Herrera Ramírez

Key Points

  • This research aims to optimize the secondary annealing parameters for improving magnetic performance in M4 grade grain-oriented electrical steel toroidal cores.
  • 32 full-factorial design varying temperature (650, 850, 1050 °C) and holding time (60, 90, 120 min) on assembled M4 cores.
  • Mechanistic analysis with SEM, EDS, and ICP-OES to assess microstructural changes and coating stability.
  • Specific losses measured before and after optimization.
  • Optimal annealing condition (850 °C, 90 min) reduced specific losses from 0.85 W/kg to 0.43 W/kg (49% reduction).
  • Primary recrystallization resulted in equiaxed grains of ~50–60 µm, contributing to enhanced performance.
  • Temperatures above 850 °C resulted in magnetic deterioration due to excessive grain growth.

Abstract

Grain-oriented (GO) silicon steel cores in low-voltage current transformers suffer magnetic degradation from residual stress and increased dislocation density during slitting and winding. This study addresses the gap in systematic optimization of secondary annealing on assembled toroidal cores using a 32 full-factorial design varying temperature (650, 850, 1050 °C) and holding time (60, 90, 120 min) on M4 grade cores. Results showed temperature is the dominant factor, while holding time exhibits a synergistic non-linear effect. The optimal condition (850 °C, 90 min) reduced specific losses from 0. 85 W/kg to 0. 43 W/kg (49% reduction). Mechanistic analysis confirmed this improvement is driven by complete primary recrystallization (equiaxed grains ~50–60 µm), dislocation annihilation (~10 HV hardness reduction), and reinforcement of the Goss texture (110). SEM, EDS, and ICP-OES demonstrated that the Carlite coating remained dimensionally (1. 67–1. 83 µm) and chemically stable, with beneficial decarburization. Temperatures above 850 °C caused magnetic deterioration due to excessive grain growth. These results provide a validated, industrial framework for recovering magnetic efficiency in wound toroidal cores without compromising coating integrity.

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Cite This Study

Moreno-Ríos et al. (2026) studied this question.

synapsesocial.com/papers/6a153bdfb5d9c58d83e8d49ahttps://doi.org/10.3390/ma19112203
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