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May 29, 2026Molbank1 citationsOpen Access

Eco-Friendly Synthesis of Perimidine Derivatives Using Recyclable Fe3O4@Nano-Cellulose/Ti(IV)

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GPGhaffar PasdarABAbdolhamid BamoniriBMBi Bi Fatemeh Mirjalili

Key Points

  • This research aims to develop a sustainable method for synthesizing perimidine derivatives using a green nanocatalyst.
  • Utilized Fe3O4@nano-cellulose/Ti(IV) as a magnetic Lewis acid nanocatalyst.
  • Characterized the catalyst using XRD, FESEM, and TGA analyses.
  • Conducted reactions in eco-friendly solvents, applying ultrasonic techniques.
  • Achieved high yields of perimidine derivatives under mild conditions.
  • The nanocatalyst showed remarkable activity and efficient magnetic recovery.
  • Maintained excellent reusability over several cycles with minimal efficiency loss.

Abstract

A novel bio-capable method has been implemented for the synthesis of newly substituted derivatives of perimidine using Fe3O4@nano-cellulose/Ti(IV) as a magnetic, sustainable, and eco-friendly Lewis acid nanocatalyst. The catalyst was thoroughly characterized by XRD, FESEM, and TGA analyses, confirming its crystalline structure, uniform nanoscale morphology, and high thermal stability. The reaction proceeded smoothly in eco-friendly solvents, providing outstanding yields under mild and rapid conditions, especially with ultrasonics. The catalyst, derived from renewable materials, exhibited remarkable activity, easy magnetic recovery, and excellent reusability over several cycles without significant loss of efficiency. Spectral characterization, IR, 1H NMR, 13C NMR, 19F NMR, and HRMS analyses verified that perimidine derivatives were synthesized properly. This sustainable and efficient approach demonstrates the prospect of green Lewis acid nanocatalysts for the sustainable synthesis of valuable heterocyclic compounds.

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Cite This Study

Pasdar et al. (2026) studied this question.

synapsesocial.com/papers/6a192e4efab5b468c4417651https://doi.org/10.3390/m2181
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