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June 3, 2026Journal of Chemometrics0 citations

Risk‐Adjusted Robust Classification of Coagulation Potential in the Regeneration of Waste Lubricant Oil

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RGRúben GarisoTRTiago J. RatoMQMargarida J. Quina

Key Points

  • The aim is to develop a robust machine learning method to predict the coagulation potential of waste lubricant oil to improve decision-making in its regeneration.
  • Developed a machine learning system based on Fourier-transform infrared spectroscopy for waste lubricant oil analysis.
  • Implemented three key modules: feature extraction, robust classification using risk-adjusted rules, and soft validation of negative predictions.
  • Initially achieved 70% accuracy with a traditional PAT-based model due to misclassification issues.
  • The proposed methodology reliably classified waste lubricant oil samples, improving upon the earlier model's accuracy.
  • Demonstrated significant reduction in laboratory workload while aiding decision-making.
  • Addressed safety risks by minimizing misclassification of coagulating waste lubricant oil.

Abstract

ABSTRACT Despite their ubiquitous presence in scientific publications and media, the number of artificial intelligence and machine learning (AI/ML) systems installed and operating in industry is still incipient. Issues such as robustness, memory requirements, maintenance, and interpretability hinder their diffusion and wider adoption. In this article, we report a system developed to operate in the circular economy of lubricant oil that cleared all of these requirements and is now under supervised adoption in industry. We also share important refinement stages that were crucial for the ML algorithm to work properly and deliver the aimed aided‐value for decision‐making. More specifically, to expedite decision‐making and mitigate safety risks, a robust classification method is proposed to predict the coagulation potential of waste lubricant oil (WLO), a hazardous waste according to the European legislation. The occurrence of the coagulation phenomena renders WLO regeneration into base oil production unfeasible. Leveraging on Fourier‐transform infrared (FTIR) spectroscopy and ML, the proposed methodology comprises three key modules: feature extraction and validation of the model, robust classification using risk‐adjusted rules, and soft validation of negative predictions. The original PAT‐based ML classification model achieved only 70% accuracy, mostly due to misclassification of WLO that coagulates, which represents the highest risk for the process operation. In turn, the proposed methodology was able to reliably classify the WLO samples, showcasing its value for decision‐making together with a significant reduction in laboratory workload.

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Cite This Study

Gariso et al. (2026) studied this question.

synapsesocial.com/papers/6a1fc6cddee9eb8c0dce7bc0https://doi.org/10.1002/cem.70150
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