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The brittleness of an aluminide diffusion coating protecting a Ren\'e 125 Ni-based polycrystalline superalloy was investigated over a wide range of temperatures in its as-received and thermally aged form. Isothermal and thermal cycled aging were performed on the coated system at a maximum temperature of 1100 C. Microstructure evolutions and damage initiation within the coating were characterized. Interrupted tensile tests and thermomechanical fatigue tests were conducted to document critical stress-strain conditions leading to the coating cracking and lifetime for the case of thermo-mechanical fatigue loading. Advanced digital image correlation and acoustic emission techniques were used to detect coating cracking. Isothermal oxidation or cyclic oxidation led to improved strain-to-failure due to metallurgical evolutions and also longer fatigue life under thermomechanical fatigue conditions.
Billard et al. (Tue,) studied this question.
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