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Stress in polycrystalline and amorphous silicon thin films deposited on oxidized silicon wafers is determined from the lengthening of the undercut edge of a silicon stripe. The technique measures only compressive stresses, has a stress resolution of 108 dyn/cm2, and a spatial resolution on the wafer of 250 μm. Unannealed silicon thin films deposited on oxide are under high compressive stress (1010 dyn/cm2). This stress is reduced below the resolution by annealing at 1100 °C for 20 min in N2, except for the thinnest polycrystalline silicon films studied (230 nm thick).
Howe et al. (Mon,) studied this question.