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This reaction generates diverse sulfonated benzo[1,3]oxazines using photocatalysis and copper catalysis, highlighting functional group tolerance.
Under light irradiation, a reaction of N ‐(2‐(prop‐1‐en‐2‐yl)phenyl)benzamides, thianthrenium salts and sodium hydrogen sulfite under copper catalysis and photocatalysis is developed. Diverse sulfonated benzo[ d ][1,3]oxazines are generated in good yields with broad functional group tolerance by using sodium hydrogen sulfite as the sulfur dioxide surrogate. During the reaction process, a radical pathway with the insertion of sulfur dioxide is proposed.
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Chen et al. (2025) studied this question.
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