This research demonstrates the synthesis and spectroscopic characteristics of thioperoxide CF3SOCH3 and its isotopologue, indicating significant conformation insights.
The elusive S -(trifluoromethyl) O -(methyl) thioperoxide, CF 3 SOCH 3 , and its methyl deuterated isotopologue, CF 3 SOCD 3 were prepared for the first time via the reaction between CF 3 SCl and CH 3 OH or CD 3 OH, respectively.
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Reina et al. (2025) studied this question.
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