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September 28, 2025ACS Applied Materials & Interfaces9 citations

Dynamic Metal-Phenolic Coordinated Hydrogel for Synergistic Photothermal/Chemodynamic Therapy against Biofilm-Infected Wounds and Real-Time Monitoring

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LLLixia LiZZZhiqin ZhaoYGYuhang Gao

Key Points

  • Synergistic therapy using mild photothermal and chemodynamic approaches achieved over 95% eradication of biofilms.
  • In vivo evaluations showed a remarkable 98.2% wound closure in 12 days due to effective bacterial elimination.
  • This hydrogel combines real-time monitoring capabilities with dynamic antibacterial properties for improved wound healing.
  • Dynamic cross-linking of quaternized chitosan with layered double hydroxides enhances adhesion and antibacterial effectiveness.

Abstract

The development of multifunctional hydrogel dressings integrating injectability, self-healing capability, tissue adhesion, multimodal antibacterial mechanisms, and real-time wound status monitoring remains a critical challenge for combating bacterial biofilms and accelerating wound healing. Herein, we present a dynamically cross-linked nanocomposite hydrogel (QCS-TA/LDH-panis) via Fe3+/Mn2+-mediated coordination between tannic acid (TA)-modified quaternized chitosan (QCS-TA) and polysulfonatoaniline-intercalated FeMn-layered double hydroxide (LDH-panis). The LDH-panis nanohybrids, synthesized through in situ polymerization of 3-sulfonatoaniline within FeMn-LDH interlayers, exhibit a near-infrared (NIR)-responsive photothermal effect (η = 64.3%) and pH/H2O2-activated peroxidase-like activity for biofilm-disrupting hydroxyl radical (•OH) generation. Concurrently, the QCS-TA matrix enables a "capture-and-kill" mechanism via electrostatic interactions (quaternary ammonium groups) and bacterial affinity adhesion (catechol/pyrogallol moieties). Under near-infrared (NIR) irradiation, synergistic mild photothermal/chemodynamic therapy (mPTT/CDT) combined with contact-killing achieved >95% eradication of Staphylococcus aureus and Escherichia coli biofilms. Notably, the hydrogel's conductivity enabled real-time monitoring of wound exudate and temperature fluctuation during the healing progression. In vivo evaluations confirmed accelerated infected wound regeneration (98.2% closure in 12 days) through biofilm elimination, inflammatory suppression, reepithelialization, and collagen deposition. This multifunctional hydrogel unifies dynamic adaptability, multimodal antibacterial therapy, and sensing intelligence, offering a promising strategy for the clinical management of biofilm-associated infection.

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Cite This Study

Li et al. (2025) studied this question.

synapsesocial.com/papers/68d90a0141e1c178a14f617bhttps://doi.org/10.1021/acsami.5c17481
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