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October 16, 2025Polymers2 citationsOpen Access

Analysis of the Effect of Transition-Metal Oxide Content on Reducing the Flammability of Polypropylene

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JIJacek IwkoBABeata AnwajlerRWRoman Wróblewski

Key Points

  • As little as 0.25 wt.% of zinc oxide increases the LOI of polypropylene to 30%, improving its flammability rating.
  • Mechanical testing reveals that titanium oxides enhance stiffness by about 15% and flexural strength by approximately 20% without significant loss in tensile strength.
  • The highest LOI observed was 43.7% with 1.5 wt.% zinc oxide, while manganese oxide showed a linear increase, achieving 38.6% at 2 wt.%.
  • The study demonstrated that the incorporation of small amounts of these oxide additives can balance flame retardancy with mechanical performance in polypropylene composites.

Abstract

Polypropylene (PP) exhibits high flammability (LOI ≈ 17.5%), which limits its industrial applications. Previous studies have primarily focused on the flame-retardant mechanisms of intumescent flame-retardant (IFR) systems, while less attention has been given to the role of inorganic synergistic additives in balancing flame retardancy with mechanical performance—an aspect crucial for commercial applications This study investigated the effect of small additions of zinc oxide (ZnO) and manganese oxide (MnO) on the flame-retardant, mechanical, and thermal properties of PP/IFR (APP + PER) composites. The oxide content was varied between 0 and 2 wt.%. LOI and UL-94 tests showed that as little as 0.25 wt.% increased LOI to 30% and enabled all materials to achieve a UL-94 V-0 classification. The highest performance was observed for ZnO (LOI = 43.7% at 1.5 wt.%), while MnO induced a linear increase up to 38.6% at 2 wt.%. SEM analysis confirmed the formation of a compact, foamed char layer. Mechanical testing revealed improved stiffness (~15%) and flexural strength (~20%), with unchanged tensile strength but reduced impact strength (−50% for ZnO, −30% for MnO). The HDT increased from 55 °C to 65 °C. These findings demonstrate that small amounts of ZnO and MnO act as effective and economically viable IFR synergists in PP composites.

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Cite This Study

Iwko et al. (2025) studied this question.

synapsesocial.com/papers/68f04927e559138a1a06dde7https://doi.org/10.3390/polym17202734
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