The synthesis of fine W composite powder with homogeneously dispersed Cu particles was investigated. Commercial or ultrasonic spray pyrolysis WO3 powders were used as source materials of W, and copper nitrate was added and hydrogen-reduced to finally fabricate W-Cu composite powder. The reduced powder prepared using ultrasonic spray pyrolysis WO3 powder exhibited a spherical agglomerate composed of fine particles and pores, whereas that using commercial WO3 showed relatively fine particles with a size of about 200 nm. TEM analysis revealed that Cu elements were uniformly distributed in the composite powder. These results help to optimize the synthesis process of homogeneous W-Cu nanocomposite powders.
Choi et al. (Tue,) studied this question.