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December 6, 2025The Journal of Organic Chemistry2 citations

Computational Study on Data Integration in Chiral Catalyst Design: A Case Study Using Michael Addition Reactions

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SYShigeru Yamaguchi

Key Points

  • Enantioselectivity improved across seven catalytic systems through integrated data analysis with DFT methods.
  • Regression analysis used free energy relationships derived from diverse transition-state structures.
  • Assessment of various chiral catalyst designs involved data integration in coordination with Michael addition reactions.
  • Findings highlight new capabilities in molecular catalysis, pointing to the need for further exploration in data-driven approaches.

Abstract

Data science in molecular catalysis often relies on the idea that molecules with similar structures show similar properties. This concept underlies many successful examples of regression analysis based on free energy relationships, typically using data sets in which substituents are varied on a single catalyst or substrate scaffold. Here, we present data integration for chiral catalyst design via regression using three-dimensional image-like descriptors (voxel data) derived from 718 TS (transition-state) structures calculated through DFT methods, along with their corresponding computed ΔΔG‡ values (energy differences between TSs leading to each enantiomer). These data sets covered seven reaction types, including organocatalysis, transition-metal catalysis, and both Michael addition and Diels-Alder reactions. Regression using integrated data sets from seven pairs of distinct reaction systems enabled the design of chiral catalysts with improved computed enantioselectivity in all seven catalytic systems. To facilitate applications, we have released a web platform (https://mcds.riken.jp) that offers a data-driven design tool and a database of DFT-computed TS data.

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Shigeru Yamaguchi (2025) studied this question.

synapsesocial.com/papers/69337cefb3f947a0a125a489https://doi.org/10.1021/acs.joc.5c02438
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