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This research demonstrates regioselective bond formation in styrenes through photoredox-catalyzed processes, highlighting new synthetic possibilities.
Based on our previous work, a photoredox-catalyzed transfer thiobenzoyloxylation of styrenes using oxime-based surrogates is reported. The redox-neutral protocol enables regioselective vicinal C–S and C–O bond formation under mild conditions. Mechanistic studies support a radical–polar crossover pathway.
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Bicic et al. (2026) studied this question.
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