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X-ray absorption spectroscopy examines size effects on local structure in nanophase palladium, indicating new insights.
The connection between local structure and the grain size distribution in nanophase palladium is studied by X-ray absorption spectroscopy (XAFS) and X-ray diffraction. XAFS shows that there is a reduced average coordination number in all samples; this reduction is compatible with a size effect, contradicting previous XAFS measurements.
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D' et al. (1995) studied this question.
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