This protocol demonstrates the synthesis of medium-ring benzolactams using nickel catalysis, suggesting a novel approach in organic synthesis.
A protocol of denitrogenative re-cyclization of benzotriazinones with di(pseudo)haloalkanes via tandem Ni-catalyzed, Mnmediated intermolecular cross-electrophile coupling / intramolecular N-alkylation is reported for access to a variety of tetrahydrobenzoazepin-1-ones and tetrahydrobenzoazocin-1(2H)-ones....
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Xiao et al. (2026) studied this question.
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