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March 13, 2026ACS CatalysisOpen Access

Dual-Ligand System for Mild Decarbonylative Suzuki–Miyaura Cross-Coupling of Aroyl Chlorides

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Authors

MSMarcus H. SakYJYichen JiangEJEric N. Jacobsen

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Overview

Experimental and computational studies demonstrate improved yield and selectivity in cross-coupling reactions using a dual-ligand system, suggesting new catalytic methods.

Key Points

  • This research aims to establish how a dual-ligand system improves decarbonylative Suzuki–Miyaura cross-couplings.
  • Utilized a pair of phosphine ligands in palladium-catalyzed reactions.
  • Performed both experimental and computational studies.
  • Investigated the ligand-relay mechanism for enhanced performance.
  • Achieved improved yields and selectivity in reactions compared to using single ligands.
  • Validated the efficacy of pooling-deconvolution screening method for identifying catalytic mechanisms.
  • Demonstrated cooperativity between ligands enhances reaction efficiency.

Cite This Study

Sak et al. (2026) studied this question.

synapsesocial.com/papers/69b3ac6002a1e69014cce06ahttps://doi.org/10.1021/acscatal.5c08167
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