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March 21, 2026Separations2 citationsOpen Access

Macroporous Resin-Based Purification of Flavonoids: Quantitative Structure–Adsorption Relationships and a Preliminarily Validated Selection Framework

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GTGang TianYTYe TianSCShiping Cheng

Key Points

  • The aim is to create a structured approach for selecting macroporous resins based on flavonoid characteristics.
  • Conducted a systematic literature review across major scientific databases from January 2000 to February 2026.
  • Identified and synthesized findings from 55 studies on flavonoid adsorption.
  • Categorized flavonoids into operational classes based on resin polarity and adsorption characteristics.
  • Non-polar resins preferred less polar aglycones and methoxylated flavonoids.
  • Medium-polar and polar resins were more effective for glycosylated or hydrophilic flavonoids.
  • Developed a framework for resin prioritization that enhances initial screening for various flavonoid types.

Abstract

Macroporous adsorption resins (MARs) are widely used for preparative-scale flavonoid purification, yet rational resin selection remains difficult because flavonoids differ substantially in hydrophobicity, hydrogen-bonding capacity, molecular size, and planarity. This review reorganizes the available literature into a structure-guided and data-supported selection aid rather than a fully predictive model. A systematic search of Web of Science, Scopus, PubMed, and CNKI (January 2000 to February 2026) identified 55 studies for qualitative synthesis. Because many reports describe total flavonoids or mixed extracts rather than explicit single-compound adsorption data, only the subset with sufficiently clear compound-level or narrowly interpretable adsorption information was used for cautious comparative interpretation. Across the compiled evidence, non-polar resins generally favored less polar aglycones and methoxylated flavonoids, whereas medium-polar and polar resins more often performed well for glycosylated or more hydrophilic targets. On this basis, flavonoids were organized into four operational classes linked to recommended resin polarity, indicative adsorption capacity ranges, and typical ethanol-elution windows. A retrospective comparison with independent literature cases suggests practical value for initial resin prioritization, but the framework should be interpreted primarily as a heuristic, trend-based guide rather than as a strictly predictive model, because mixed-matrix effects, pore accessibility, and competitive adsorption can override simple polarity matching. A generalized operating window for adsorption and desorption is also summarized. Overall, this review provides a mechanism-informed starting point for resin screening while making explicit the conditions under which case-specific experiments remain necessary.

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Cite This Study

Tian et al. (2026) studied this question.

synapsesocial.com/papers/69be35e66e48c4981c674783https://doi.org/10.3390/separations13030098
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