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April 3, 2026Angewandte Chemie International Edition2 citations

Symmetry‐Breaking Modulation of Platinum Sites in Multicomponent Alloy for Efficient Oxygen Reduction Reaction

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XSXinyi ShenXZXue ZhangWHWei Hu

Key Points

  • The aim is to understand how atomic-level interactions in a platinum multicomponent alloy affect its catalytic performance for oxygen reduction reactions.
  • Developed a PtFeCoCu multicomponent alloy with symmetry-breaking features.
  • Analyzed the alloy's atomic-level interactions and structural properties.
  • Evaluated the performance in oxygen reduction reactions under specific conditions.
  • Achieved a half-wave potential of 0.95 V<sub>RHE</sub> and mass activity of 3.53 A mg<sub>Pt</sub> <sup>-1</sup> at 0.9 V<sub>RHE</sub>.
  • Delivered a mass activity of 1.63 A mg<sub>Pt</sub> <sup>-1</sup> in an H<sub>2</sub>-O<sub>2</sub> fuel cell at 0.9 V<sub>iR-free</sub>.
  • Retained 87.7% of the initial mass activity after 30,000 cycles.

Abstract

Understanding and controlling atomic-level interactions within multicomponent alloys provides a promising avenue to drive multistep tandem catalysis. Herein, we develop an atomic symmetry-breaking PtFeCoCu multicomponent alloy that disrupts long-range order and local coordination homogeneity and identify the nature of its enhanced performance for oxygen reduction reaction (ORR). The deliberate symmetry breaking, featured by heterogeneous local coordination and anisotropic strain, enriches the Pt environment with additional transition-metal neighbors. These distortions activate multicomponent interactions and tune the Pt electronic structure, promoting ORR intermediate conversion while suppressing component dissolution. Consequently, PtFeCoCu reaches a half-wave potential of 0.95 VRHE and a mass activity of 3.53 A mgPt -1 at 0.9 VRHE in ORR. In an H2-O2 fuel cell, it delivers a high mass activity of 1.63 A mgPt -1 at 0.9 ViR-free, retaining 87.7% of its initial mass activity after 30,000 cycles. Our findings highlight symmetry breaking as a key driver with broad implications across multicomponent alloys.

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Cite This Study

Shen et al. (2026) studied this question.

synapsesocial.com/papers/69cf5d775a333a821460b477https://doi.org/10.1002/anie.5938299
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