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April 5, 2026ACS Applied Nano Materials0 citations

Gradient Assembly Approach for Fabricating MXene-Based Dual-Responsive Soft Actuators

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QZQian ZhaoGZGeorge ZhangBMBo Ma

Key Points

  • To develop a robust and stable dual-responsive soft actuator using a gradient assembly approach with MXene and PMMA nanospheres.
  • Developed gradient assembly approach to create actuators with MXene and PMMA nanospheres.
  • Prepared asymmetric structures with varying compositions along the vertical direction of the film.
  • Tested actuation performance under humidity and light stimuli, measuring bending angles and response times.
  • Achieved bending angles of up to 345° under humidity and 235° under light stimuli.
  • Measured quick response and recovery times of 45 seconds for humidity and 30 seconds for light.
  • Demonstrated stable performance over 1000 cycles without degradation.

Abstract

Soft actuators based on bilayer–multilayer structures are highly promising for the development of soft robotics. However, their long-term operational stability is often undermined by poor interlayer adhesion between different component materials. Herein, instead of adopting traditional bilayer/multilayer structures, we developed a gradient assembly approach for MXene and poly(methyl methacrylate) (PMMA) nanospheres to prepare robust humidity/light dual-responsive actuators. The gradient distribution of PMMA nanospheres along the normal direction of the MXene film yields an asymmetric structure with one side composed primarily of MXene nanosheets and the other side enriched with PMMA nanospheres. Benefiting from the asymmetric hygroscopic swelling and thermal expansion behaviors of the two sides, the composite film demonstrates reversible and rapid dual-responsive bending deformation along with outstanding long-term stability. Remarkably, the actuator exhibits a large bending angle of up to 345° under humidity stimulation and 235° under light irradiation, with fast response/recovery times of 45 ± 0.78/46 ± 0.66 s for humidity actuation and 30 ± 0.88/43 ± 0.74 s for light actuation. Moreover, it maintains excellent stability without performance degradation after 1000 cyclic actuations under both stimuli. Based on its controllable dual-response behavior, we prepared a petal mimetic actuator, a bidirectional smart switch, and a smart gripper for humidity–light synergistic manipulation, providing a design concept for soft robotics.

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Cite This Study

Zhao et al. (2026) studied this question.

synapsesocial.com/papers/69d1fc28a79560c99a0a1d5ehttps://doi.org/10.1021/acsanm.6c00600
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