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Methoxyisocyanate ( 1 ) can be prepared by photolysis of methyl azidoformate ( 3 ) or pyrolysis of N ‐methoxycarbonyl‐ O ‐methyl‐hydroxylamine ( 4 ). Aminoisocyanate ( 2 ) is similarly formed on photolysis of carbamoyl azide ( 12 ) and pyrolysis of either methyl carbazate ( 13 ) or 3,4‐diaminofurazan ( 14 ). The infrared spectra of 1 and 2 in an argon matrix at 10 K have been measured, and some of their properties are discussed.
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Teles et al. (1989) studied this question.
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