A new complex containing the {OVv(μ-O)VvO}4+ unit has been synthesized and structurally characterized. Cyclic voltammogram of this complex showed that the two VV centers of the V2O34+ core are found to undergo electrochemical reduction in two distinctly separate steps not observed previously in similar systems. A rare mixed-oxidation state species [L(O)VIVOVV(O)L]- has been electrogenerated from the structurally characterized parent divanadium (V) species in solution state and characterized by IR, EPR, and electronic spectroscopy.
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Dinda et al. (2002) studied this question.
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