Amorphous calcium carbonate is produced as spherical particles (see Figure) via in‐situ generation of CO 2 by hydrolysis of dialkyl carbonates in aqueous solution of CaCl 2 at room temperature. This method of synthesis (precipitation) allows detailed studies of the particle formation process. Temperature‐dependent results are rationalized in terms of a phase diagram that assumes a liquid–liquid immiscibility gap with a lower critical separation temperature.
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Faatz et al. (2004) studied this question.
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