Reaction of TmI2(THF)x with the bulky scorpionate, KTptBu,Me, gave (TptBu,Me)TmI(THF) (1). Complex 1 proved to be a useful starting material for a select number of heteroleptic Tm(II) compounds, (TptBu,Me)TmER, including the first Tm(II)-hydrocarbyl derivative, (TptBu,Me)Tm{CH(SiMe3)2} (2).
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Cheng et al. (2008) studied this question.
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