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May 17, 2026Crystals0 citationsOpen Access

Microstructural Evaluation of Plasma-Vitrified Wind Turbine Blade Slag and Its Alternative Application in Geopolymer

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VSVilma SnapkauskienėRKRegina Kalpokaite-DickuvieneABArūnas Baltušnikas

Key Points

  • This study aims to evaluate plasma-vitrified wind turbine blade waste for its potential use in geopolymer materials.
  • Plasma vitrification at 2750 K converted wind turbine blade waste into a reactive slag.
  • Characterization techniques included X-ray diffraction, Fourier transform infrared spectroscopy, and scanning electron microscopy.
  • Chemical stability tests assessed dissolution behavior in acidic and alkaline media.
  • Vitrified slag comprised 30–89% amorphous phase and 10–55% anorthite according to sampling locations.
  • Addition of 5 wt.% slag to acid-based geopolymers resulted in a 35% decrease in mechanical strength.
  • Using metakaolin with illite impurities maintained strength similar to reference geopolymers.

Abstract

With the rapid expansion of wind energy infrastructure, there is an increasing accumulation of wind turbine blade waste (WTBW), which is mainly composed of glass fiber-reinforced thermosetting composites. Due to the irreversible nature of polymer crosslinking, conventional recycling methods remain limited. In this study, plasma vitrification was employed to convert WTBW into a reactive calcium-aluminum-silicate slag suitable for use in geopolymer materials. Plasma treatment at a temperature of approximately 2750 K resulted in the formation of predominantly amorphous vitrified slag (VS). Structural characterization using X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), and scanning electron microscopy with energy-dispersive X-ray spectroscopy (SEM-EDS) revealed the spatial heterogeneity of the VS. This heterogeneity was influenced by thermal gradients and varied between samples collected from different slag discharge zones, both vertically and horizontally from the reactor. All VS samples contained between 30 and 89% amorphous phase and 10–55% anorthite, with the proportions varying by sampling location. Chemical stability tests showed the dissolution of calcium and aluminum in acidic media, resulting in a silica-enriched residual structure in which the Ca and Al content decreased to less than 0.5 at.% after 100 days. In contrast, exposure to alkaline media caused only minimal surface reorganization—the addition of 5 wt.% VS to acid-based geopolymers made with two metakaolin precursors resulted in a 35% decrease in the mechanical strength of pure metakaolin-based systems. In contrast, when metakaolin containing illite impurities was used, strength values were similar to those of the reference geopolymer. The results quantitatively demonstrate that plasma-derived slag exhibits composition-dependent reactivity, directly linked to its amorphous content and dissolution behavior.

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Cite This Study

Snapkauskienė et al. (2026) studied this question.

synapsesocial.com/papers/6a095c037880e6d24efe1eebhttps://doi.org/10.3390/cryst16050334
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