External oxidant-free cross-coupling: electrochemically induced aromatic C–H phosphonation of azoles with dialkyl-H-phosphonates under silver catalysis

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Electrochemical catalytic oxidation with 1% silver salts enables the external oxidant-free phosphorylation of azole derivatives by dialkyl-H-phosphonates. Novelty: ClaimNovelty.METHODOLOGICAL. Consensus alignment: ConsensusAlignment.NEUTRAL.

E. O. Yurko; Tatyana V. Gryaznova; Kirill V. Kholin; Vera V. Khrizanforova; Yulia H. Budnikova

doi:10.1039/c7dt03650g

November 21, 2017Dalton TransactionsOpen Access

External oxidant-free cross-coupling: electrochemically induced aromatic C–H phosphonation of azoles with dialkyl-H-phosphonates under silver catalysis

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Abstract

A convenient external oxidant-free method of azole derivatives phosphorylation by dialkyl-H-phosphonates through electrochemical catalytic oxidation in the presence of silver salts (1%) is proposed.

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Yurko et al. (2017) studied this question.

synapsesocial.com/papers/6a0b9af7faed69294fd0a49b https://doi.org/10.1039/c7dt03650g

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External oxidant-free cross-coupling: electrochemically induced aromatic C–H phosphonation of azoles with dialkyl-H-phosphonates under silver catalysis

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External oxidant-free cross-coupling: electrochemically induced aromatic C–H phosphonation of azoles with dialkyl-H-phosphonates under silver catalysis

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