Robust single-scan ultraselective NMR

Margherita Bazzoni; Armand Régheasse; Patrick Giraudeau; Aurélie Bernard; Ralph W. Adams; Gareth A. Morris; Mathias Nilsson; Peter Kiraly; Jean‐Nicolas Dumez

doi:10.1039/d6cc01693f

January 1, 2026Chemical Communications

Robust single-scan ultraselective NMR

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Key Points

This research aims to enhance the sensitivity of GEMSTONE NMR experiments for selecting overlapping 1H multiplets.
Developed a robust single-scan ultraselective GEMSTONE NMR technique.
Focused on optimizing sensitivity against relaxation and diffusion losses.
Utilized advanced data processing algorithms for improved selection efficacy.
Achieved significant sensitivity improvements compared to standard GEMSTONE methods.
Demonstrated effective selection of overlapping multiplets with minimal signal loss.
Validated the technique across various sample types, enhancing practical applications.

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Abstract

Single-scan ultraselective GEMSTONE NMR experiments efficiently select 1H multiplets that partially overlap with other multiplets. However, current implementations of GEMSTONE can suffer significant sensitivity losses due to relaxation and diffusion....

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Bazzoni et al. (2026) studied this question.

synapsesocial.com/papers/6a17dbe93fad632b0f9d8931 https://doi.org/10.1039/d6cc01693f

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Robust single-scan ultraselective NMR

Key Points

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Abstract

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Robust single-scan ultraselective NMR

Key Points

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Abstract

Discussion

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