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Mechanistic study reveals advantages of C(sp2)–H sulfonylmethylation in various compounds, indicating a new method's efficiency.
-dimethylaniline. Tetramethylolglycoluril acts as an in situ C1 source and is required in substoichiometric amounts. Mechanistic studies suggest an ionic mechanism for the reaction. Easy operation, broad substrate scope, and reusable solvent are a few advantages of the developed methodology.
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Chillal et al. (2026) studied this question.
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