GdFe and TbFe films sputtered with substrate bias voltage (VB) have been annealed both in air and in vacuum at temperatures up to 300°C In the case of annealing in air the oxidation occurs at the film surface and forms an oxidized layer that has in-plane magnetization,and therefore, the perpendicular anisotropy (Ku) decreases. Crystallographic structure of the films changes from the amorphous state into crystal-like one with increasing VB. The amorphous films sputtered with low VB oxidize more readily than the crystal-like films. Consequently the films sputtered with low VB show a larger decrease in Ku than those with high VB. Annealing in vacuum does not seem to change the film properties.
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Nawate et al. (1985) studied this question.
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