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High-field 51V and 17O n.m.r. spectroscopy has clarified the aqueous chemistry of the peroxovanadates, leading to the identification of five new species, four of which are dimeric, Mono- and di-peroxovanadates undergo a change of co-ordination from octahedral to tetrahedral when their final proton is removed.
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Harrison et al. (1985) studied this question.
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