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Abstract A new shelf‐stable and easily scalable difluoromethylthiolating reagent S ‐(difluoromethyl) benzenesulfonothioate (PhSO 2 SCF 2 H) was developed. PhSO 2 SCF 2 H is a powerful reagent for radical difluoromethylthiolation of aryl and alkyl boronic acids, decarboxylative difluoromethylthiolation of aliphatic acids, and a phenylsulfonyl‐difluoromethylthio difunctionalization of alkenes under mild reaction conditions.
Zhu et al. (Thu,) studied this question.
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