Raman spectroscopy is found to be a powerful tool to determine the structural phase boundary between cubic (Fm3m) and tetragonal (P42/nmc) phase in arc-melted Zr1−XYXO2−X/2 (0.08≤X≤0.24) solid solution. The Raman peak intensity characteristic of the tetragonal phase at about 470 cm−1 decreases with the YO1.5 content X and becomes 0 around X=0.18.
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Yashima et al. (1993) studied this question.
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