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The aggregation of CuS nanoparticles during synthesis by a hassle-free aqueous route under microwave irradiation gave remarkable spherical shape, utilizing Cu(CH3COO)2·H2O as the source of copper and Na2S2O3·5H2O, as sulfur source; these materials were used without assistance of any surfactant or template. An X-ray powder diffraction pattern proved that the product is hexagonal CuS phase. The morphologies of the product were observed by scanning electron microscopy. Thermal behavior, different solid state, and chemical conversion in CuS with respect to temperature were studied by DSC/TGA, which confirmed the thermal oxidation of CuS and its conversion into CuO then to Cu2O.
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Nafees et al. (2012) studied this question.
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